文章摘要
刘 佳, 李 琼, 黄惠芳,等.海南黄灯笼辣椒油树脂的超临界CO2提取工艺优化及GC-MS分析[J].广东农业科学,2015,42(6):74-79
查看全文    HTML 海南黄灯笼辣椒油树脂的超临界CO2提取工艺优化及GC-MS分析
Optimization of oleoresin extraction from HainanCapsicum chinense by supercritical CO2 andanalysis on capsicum oleoresin by GC-MS
  
DOI:
中文关键词: 海南黄灯笼辣椒  超临界 CO2萃取  HPLC 法  气相色谱-质谱法
英文关键词: Capsicum chinense  supercritical CO2 method  high performance liquid chromatograph method  gaschromatography-mass spectrometry
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作者单位
刘 佳, 李 琼, 黄惠芳,等 .海南大学农学院中国热带农业科学院热带作物品种资源研究所广西壮族自治区亚热带作物研究所 
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中文摘要:
      以海南黄灯笼辣椒粉为原料,采用超临界 CO2萃取法提取辣椒油树脂,并采用 GC-MS 法对辣椒 油树脂成分进行分析。正交试验结果表明,以辣椒油树脂得率为标准,最优化的提取条件为:压力 23 MPa,温度 47益,流量 35 L/h,时间 90 min;以辣椒素提取率为标准,最优的提取条件为:压力 23 MPa,温度 50益,流量 45 L/h,时间 90 min。 利用 GC-MS 分析黄灯笼辣椒油树脂,共检出 27 组化合物,主要化合物含量由高到低依次为 辣椒素类物质(31.64%)、亚油酸(6.64%)、棕榈酸(4.84%)、反式肉桂醛(4.765%)、正二十七烷(1.675%)、芳姜黄 酮(1.375%)、反式角鲨烯(1.325%)、茁-谷甾醇(1.115%)、亚油酸甘油酯(1.075%)。
英文摘要:
      Supercritical CO2 method was used to optimize the extraction conditions of oleoresin from Capsicum chinense in Hainan Province, and gaschromatography -mass spectrometry method was used to determine the compoments of the oleoresin. The results demonstrated that the optimum extraction conditions to get more capsicum oleoresin were confirmed as follows: pressure of 23 MPa, temperature of 47℃, flow rate of 35 L/h for 90 min. While the optimum extraction conditions to get higher extraction rate were confirmed as follows: pressure of 23 MPa, temperature of 50℃, flow rate of 45 L/h for 90 min. 27 kinds of compounds were identified by GC-MS in capsicum oleoresin, and the major compounds were capsaicin (31.64%), linoleic acid (6.64%), palmitic acid (4.84%), trans cinnamic aldehyde (4.765%), heptacosane (1.675%), aromatic ginger flavonoids (1.375%), trans squalene (1.325%), beta sitosterol (1.115%), linoleic acid glycerol ester (1.075%).
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