文章摘要
Optimization and detection of microcytin in drinkingwater using solid phase extraction-highperformance liquid chromatography
  
DOI:
Author NameAffiliation
郭伟 黑亮 杨燕婷 雷列辉 朱小平 珠江水利委员会珠江水利科学研究院广东广州510611 
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Abstract:
      This study established an available analysis method for the detection of microcystin LR in drinking water. The mobile phase acidity, elution rate and column temperature were optimized in this method. 0.04% TFA/acetonitrile (63 37) was chosen as the mobile phase, elution time was 7 min. The method was gentle, fast, economical, available etc. Through the detection and analysis of microcystin LR in a typical reservoir of Guangdong province, we found that this method was reliable, accurate, sensitive, and the recovery was 88%, the lowest detection limit was 0.05 g/L.
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